Investigation of the effect of sintering temperature on structural, magnetic and magnetocaloric properties in PrCaMn2O6 double perovskite manganite system

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dc.authoridEkicibil, Ahmet/0000-0003-3071-0444
dc.authoridAkca, Gonul/0000-0001-7187-9516
dc.authoridAYAS, Ali Osman/0000-0002-6186-8191
dc.authoridKandemir, Arda/0000-0002-9439-0366
dc.contributor.authorAyas, Ali Osman
dc.contributor.authorKandemir, Arda
dc.contributor.authorCetin, Selda Kılıç
dc.contributor.authorAkca, Gonul
dc.contributor.authorAkyol, Mustafa
dc.contributor.authorEkicibil, Ahmet
dc.date.accessioned2025-01-06T17:44:55Z
dc.date.available2025-01-06T17:44:55Z
dc.date.issued2022
dc.description.abstractWe have studied the effect of sintering temperature change on structural, magnetic and magnetocaloric properties of PrCaMn2O6 compound. The samples were produced by using solid-state-reaction process and then sintered at 1000, 1100 and 1200 degrees C temperatures. The Rietveld refinement results indicate that the crystal symmetry of the produced samples is tetragonal with P4mm space group. All samples include impurity phase, and their percentages decrease with increasing sintering temperature. Scanning electron Microscope images show that grain sizes of samples increase with increasing T-S. Energy-dispersive X-ray spectra indicate that samples include all required starting elements. Temperature-dependent magnetization measurements show that samples have the Curie temperatures as 42.6, 43.1, and 42.8 K for samples sintered at 1000, 1100 and 1200 degrees C, respectively. Magnetic entropy change values are found as 1.19, 1.59 and 1.72 J kg(-1) K-1 at 5 T magnetic field change for samples sintered at 1000, 1100 and 1200 degrees C, respectively. Relative cooling power values are calculated as 14.28, 20.54 and 17.20 J kg(-1) for samples sintered at 1000, 1100 and 1200 degrees C, respectively. The universal curve and the Arrott plots show that magnetic phase transition type of all samples is second order.
dc.description.sponsorshipTUBITAK (The Scientific and Technological Research Council of Turkey) [120M409]
dc.description.sponsorshipThis work is supported by the TUBITAK (The Scientific and Technological Research Council of Turkey) Under Grant Contract no 120M409.
dc.identifier.doi10.1007/s10854-022-07843-4
dc.identifier.endpage7370
dc.identifier.issn0957-4522
dc.identifier.issn1573-482X
dc.identifier.issue10
dc.identifier.scopus2-s2.0-85125278531
dc.identifier.scopusqualityQ2
dc.identifier.startpage7357
dc.identifier.urihttps://doi.org/10.1007/s10854-022-07843-4
dc.identifier.urihttps://hdl.handle.net/20.500.14669/3242
dc.identifier.volume33
dc.identifier.wosWOS:000761897700003
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofJournal of Materials Science-Materials in Electronics
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241211
dc.subjectCrystallography Open Database
dc.subjectOpen-Access Collectıon
dc.subjectPhase-Transıtıons
dc.subjectDouble-Exchange
dc.subjectBehavıor
dc.titleInvestigation of the effect of sintering temperature on structural, magnetic and magnetocaloric properties in PrCaMn2O6 double perovskite manganite system
dc.typeArticle

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