Production of NiCoMo-Supported Ni Foam for Electrocatalytic Oxidation of Methanol: Experimental and RSM Analysis

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dc.authoridGungor, CEYLA/0000-0002-4072-6784
dc.authoridDogru Mert, Basak/0000-0002-2270-9032
dc.authoridMERT, MEHMET ERMAN/0000-0002-0114-8707
dc.contributor.authorMert, Basak Dogru
dc.contributor.authorDemir, Beyza Nur
dc.contributor.authorEdis, Cansu
dc.contributor.authorAkyildiz, Senay
dc.contributor.authorOzgur, Ceyla
dc.contributor.authorMert, Mehmet Erman
dc.date.accessioned2025-01-06T17:43:35Z
dc.date.available2025-01-06T17:43:35Z
dc.date.issued2024
dc.description.abstractThe Ni-, Co-, and Mo-supported Ni foam (NiF-NiCoMo) was produced via galvanostatic method, and electrooxidation of methanol in alkaline medium was examined. The characterization was achieved using field emission scanning electron microscopy, energy-dispersive X-ray, and X-ray diffraction analysis. The electrochemical behavior was determined via cyclic voltammetry and chronoamperometry analysis. The contribution of each transition metal to electrocatalytic performance of NiF was monitored via mono, binary, and ternary modifications of each transition metal (Ni, Co, and Mo) for several amounts (5, 10, and 15 mu g). Experiments were performed to determine the influence of catalyst amounts, methanol concentration, and scan rate parameters. The impacts of independent parameters on methanol electrooxidation were statistically investigated using Design-Expert software. The ability to analyze multiple parameters with a limited number of experimental performances is one of the method's key benefits. The developed model showed that 9.41 and 14.03 mu g catalyst amounts were the appropriate values for NiF-NiMo and NiF-NiCoMo achieving optimal circumstances, respectively.
dc.description.sponsorshipScientific and Technological Research Council of Turkiye (TUB ITAK)
dc.description.sponsorshipOpen access funding provided by the Scientific and Technological Research Council of Turkiye (TUB ITAK).
dc.identifier.doi10.1007/s13369-024-08905-x
dc.identifier.endpage9533
dc.identifier.issn2193-567X
dc.identifier.issn2191-4281
dc.identifier.issue7
dc.identifier.scopus2-s2.0-85189018505
dc.identifier.scopusqualityQ1
dc.identifier.startpage9517
dc.identifier.urihttps://doi.org/10.1007/s13369-024-08905-x
dc.identifier.urihttps://hdl.handle.net/20.500.14669/2725
dc.identifier.volume49
dc.identifier.wosWOS:001191042400003
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer Heidelberg
dc.relation.ispartofArabian Journal For Science and Engineering
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.snmzKA_20241211
dc.subjectMethanol electrooxidation
dc.subjectTransition metal-based catalyst
dc.subjectRSM
dc.subjectPrediction
dc.subjectOptimization
dc.titleProduction of NiCoMo-Supported Ni Foam for Electrocatalytic Oxidation of Methanol: Experimental and RSM Analysis
dc.typeArticle

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