Effect of Synthesizing Process on the Formation of Fe3O4 Magnetic Nanoparticles

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dc.contributor.authorAka, Cemal
dc.contributor.authorAkyol, Mustafa
dc.date.accessioned2025-01-06T17:22:40Z
dc.date.available2025-01-06T17:22:40Z
dc.date.issued2023
dc.departmentAdana Alparslan Türkeş Bilim ve Teknoloji Üniversitesi
dc.description.abstractIn this work, the effect of synthesizing process on the morphology, structure, and magnetic properties of Fe3O4 magnetic nanoparticles have been studied by performing X-ray diffraction, scanning electronic microscopy, and vibrating sample magnetometer measurements. Fe3O4 nanoparticles were synthesized by hydrothermal and solvothermal methods. X-ray diffraction analysis revealed that both samples have cubic crystal phase. However, Fe2O3 impurity peaks were observed in the sample synthesized by hydrothermal method. The crystallite sizes of samples synthesized by hydrothermal and solvothermal methods were approximately 38 and 24 nm, respectively. The scanning electron microscope images show that spherical porous and cubic shape Fe3O4 nanoparticles were obtained by solvothermal and hydrothermal method, respectively. The average particle sizes of Fe3O4 samples synthesized by hydrothermal and solvothermal methods were determined as 220 and 450 nm, respectively. Both samples behave a soft ferromagnetic characteristic having almost zero coercive field. The magnetic saturation values of Fe3O4 nanoparticles synthesized by hydrothermal and solvothermal methods were determined as 28.78 and 77.31 emu/g, respectively. As a result of the characterizations, porous Fe3O4 nanoparticles synthesized by solvothermal method show better crystal structure, morphological and magnetic properties than Fe3O4 nanoparticles synthesized by hydrothermal method.
dc.identifier.doi10.17776/csj.1284327
dc.identifier.endpage509
dc.identifier.issn2587-2680
dc.identifier.issn2587-246X
dc.identifier.issue3
dc.identifier.startpage504
dc.identifier.trdizinid1199271
dc.identifier.urihttps://doi.org/10.17776/csj.1284327
dc.identifier.urihttps://search.trdizin.gov.tr/tr/yayin/detay/1199271
dc.identifier.urihttps://hdl.handle.net/20.500.14669/446
dc.identifier.volume44
dc.indekslendigikaynakTR-Dizin
dc.language.isoen
dc.relation.ispartofCumhuriyet Science Journal
dc.relation.publicationcategoryMakale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.snmzKA_20241211
dc.subjectFe3O4
dc.subjectHydrothermal
dc.subjectMagnetic nanoparticles
dc.subjectSolvothermal
dc.subjectMagnetic hysteresis
dc.titleEffect of Synthesizing Process on the Formation of Fe3O4 Magnetic Nanoparticles
dc.typeArticle

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